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master's thesis
Priprava membrane LaF3 postupkom taloženja La3+ i F- uz dodatak Eu(NO3)3 za FISE
diplomski rad
2018. urn:nbn:hr:167:620347
Bek, Eva
University of Split
Faculty of Chemistry and Technology
Division of Chemistry

Cite this document

Bek, E. (2018). Priprava membrane LaF3 postupkom taloženja La3+ i F- uz dodatak Eu(NO3)3 za FISE : diplomski rad (Master's thesis). Split: University of Split, Faculty of Chemistry and Technology. Retrieved from https://urn.nsk.hr/urn:nbn:hr:167:620347

Bek, Eva. "Priprava membrane LaF3 postupkom taloženja La3+ i F- uz dodatak Eu(NO3)3 za FISE : diplomski rad." Master's thesis, University of Split, Faculty of Chemistry and Technology, 2018. https://urn.nsk.hr/urn:nbn:hr:167:620347

Bek, Eva. "Priprava membrane LaF3 postupkom taloženja La3+ i F- uz dodatak Eu(NO3)3 za FISE : diplomski rad." Master's thesis, University of Split, Faculty of Chemistry and Technology, 2018. https://urn.nsk.hr/urn:nbn:hr:167:620347

Bek, E. (2018). 'Priprava membrane LaF3 postupkom taloženja La3+ i F- uz dodatak Eu(NO3)3 za FISE : diplomski rad', Master's thesis, University of Split, Faculty of Chemistry and Technology, accessed 20 November 2024, https://urn.nsk.hr/urn:nbn:hr:167:620347

Bek E. Priprava membrane LaF3 postupkom taloženja La3+ i F- uz dodatak Eu(NO3)3 za FISE : diplomski rad [Master's thesis]. Split: University of Split, Faculty of Chemistry and Technology; 2018 [cited 2024 November 20] Available at: https://urn.nsk.hr/urn:nbn:hr:167:620347

E. Bek, "Priprava membrane LaF3 postupkom taloženja La3+ i F- uz dodatak Eu(NO3)3 za FISE : diplomski rad", Master's thesis, University of Split, Faculty of Chemistry and Technology, Split, 2018. Available at: https://urn.nsk.hr/urn:nbn:hr:167:620347

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Metadata
TitlePriprava membrane LaF3 postupkom taloženja La3+ i F- uz dodatak Eu(NO3)3 za FISE : diplomski rad
Title (english)Preparation LaF3 membrane by precipitation of La3+ and F- with additiom Eu(NO3)3 for FISE : diploma thesis
AuthorEva Bek
MentorMarija Bralić (mentor)
MBZ: 119816
Committee memberJosipa Giljanović (predsjednik povjerenstva)
Committee memberAnte Prkić (član povjerenstva)
Committee memberMarija Bralić (član povjerenstva)
GranterUniversity of Split
Faculty of Chemistry and Technology
(Division of Chemistry)
Split
Defense date and country2018-10-23, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract
U ovom radu dobiven je slabo topljiv talog LaF 3 sutaloženjem NaF i La(NO 3 ) 3 s europijem. Bijeli puderasti talog sušen je u sušioniku na 60˚C. Pripravljane su membrane različitih debljina, zbog veće čvrstoće u membrane dodavan je teflon. Odzivne karakteristike elektrode ispitivane su metodom slijednog razrijeđenja počevši od koncentracije fluorida 10 -1 do 10 -7 molL -1 . Kako bi se dobile bolje odzivne karakteristike na površinu membrana nanošene su nanočestice Fe x O y . Pripravljene membrane nisu pokazale očekivane odzivne karakteristike, promjena potencijala po dekadi znatno je niža od teorijske vrijednosti (59 mV) i iznosila je 15 mV. Dodatak nanočestica nije znatno poboljšalo odzivne karakteristike. Dodatak europija u različitim postotcima (0,3 %, 1%, 3%) nije znatno poboljšao odzivne karakteristike.
Abstract (english)
In the present thesis, sparingly soluble LaF 3 was obtained by precipitating NaF with La(NO 3 ) 3 with the addition of europium.The white powder-like precipitate was put in the dryer at 60˚C. The membranes of different thicknesses were prepared, after which the Teflon was added in order to make membranes harder. Response characteristics were tested by using the serial dilution method with concentrations of fluoride ranging from 10 -1 to 10 -7 molL -1 . Fe x O y nanoparticles were deposited on the membrane surfaces in order to receive better response. The prepared membranes did not show any kind of response that was expected, which is due to potential change towards decades being around 15 mV, which is much lower than the theoretical value (59 mV). The addition of europium ofdifferent percentages (0,3%, 1% and 3%) did not significantly improve response characteristics of membranes.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:167:620347
Study programmeTitle: Chemistry; specializations in: Environmental Protection, Organic Chemistry and Biochemistry
Course: Environmental Protection
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra kemije (magistar/magistra kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Terms of useLicence In copyright icon
Public noteKljučne riječi doradio knjižničar/ Key words are revised by the librarian
Created on2019-06-28 11:19:05