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undergraduate thesis
Određivanje eukaliptola (1,8-cineola) u eteričnim uljima mirte, kajeputa i niauli
završni rad
2022. urn:nbn:hr:167:961037
Boras, Dorja
University of Split
Faculty of Chemistry and Technology
Division of Chemistry

Cite this document

Boras, D. (2022). Određivanje eukaliptola (1,8-cineola) u eteričnim uljima mirte, kajeputa i niauli : završni rad (Undergraduate thesis). Split: University of Split, Faculty of Chemistry and Technology. Retrieved from https://urn.nsk.hr/urn:nbn:hr:167:961037

Boras, Dorja. "Određivanje eukaliptola (1,8-cineola) u eteričnim uljima mirte, kajeputa i niauli : završni rad." Undergraduate thesis, University of Split, Faculty of Chemistry and Technology, 2022. https://urn.nsk.hr/urn:nbn:hr:167:961037

Boras, Dorja. "Određivanje eukaliptola (1,8-cineola) u eteričnim uljima mirte, kajeputa i niauli : završni rad." Undergraduate thesis, University of Split, Faculty of Chemistry and Technology, 2022. https://urn.nsk.hr/urn:nbn:hr:167:961037

Boras, D. (2022). 'Određivanje eukaliptola (1,8-cineola) u eteričnim uljima mirte, kajeputa i niauli : završni rad', Undergraduate thesis, University of Split, Faculty of Chemistry and Technology, accessed 19 April 2024, https://urn.nsk.hr/urn:nbn:hr:167:961037

Boras D. Određivanje eukaliptola (1,8-cineola) u eteričnim uljima mirte, kajeputa i niauli : završni rad [Undergraduate thesis]. Split: University of Split, Faculty of Chemistry and Technology; 2022 [cited 2024 April 19] Available at: https://urn.nsk.hr/urn:nbn:hr:167:961037

D. Boras, "Određivanje eukaliptola (1,8-cineola) u eteričnim uljima mirte, kajeputa i niauli : završni rad", Undergraduate thesis, University of Split, Faculty of Chemistry and Technology, Split, 2022. Available at: https://urn.nsk.hr/urn:nbn:hr:167:961037

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Metadata
TitleOdređivanje eukaliptola (1,8-cineola) u eteričnim uljima mirte, kajeputa i niauli : završni rad
Title (english)Determination of eucalyptol (1,8-cineola) in myrtle, cajeput and niaouli essential oils : bachelor thesis
AuthorDorja Boras
MentorFranko Burčul (mentor)
Committee memberMiće Jakić (predsjednik povjerenstva)
Committee memberMario Nikola Mužek (član povjerenstva)
Committee memberFranko Burčul (član povjerenstva)
GranterUniversity of Split
Faculty of Chemistry and Technology
(Division of Chemistry)
Split
Defense date and country2022-09-26, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract
1,8-Cineol monoterpen je sadržan u brojnim eteričnim uljima. Zbog svoje ugodne arome i okusa, koristi se u raznim mirisima i kozmetici. Antioksidacijska i protuupalna svojstva čine ga važnim sastojkom u farmaceutskim proizvodima. U ovom radu razvijena je metoda za određivanje 1,8-cineola. Za kvantitativno i kvalitativno određivanje 1,8-cineola korištena je tehnika plinske kromatografije s tandemskom spektrometrijom masa. Korištenjem iste tehnike određene su koncentracije 1,8-cineola u eteričnim uljima kajeputa, mirte i niauli. Praćenjem MRM načina snimanja za različite signale 1,8-cineola određene su specifične reakcije prijelaza pomoću spektrometra masa s trostrukim kvadrupolom. Tako je spektrometrija masa optimizirana određivanjem energija sraza s dušikom za svaki izabrani prijelaz. Za izradu krivulja umjeravanja korišten je raspon koncentracija 50 µg mL -1 - 2000 µg mL -1 . Zadovoljeni su ispitani parametri vrednovanja metode (točnost, preciznost, specifičnost, linearnost, granice određivanja i dokazivanja). Analizom realnog uzorka eteričnih ulja primjenom navedene metode uspješno su im određene koncentracije.
Abstract (english)
1,8-Cineole monoterpene is contained in numerous essential oils. Due to its pleasant aroma and taste, it is used in various fragrances and cosmetics. Its antioxidant and anti-inflammatory properties make it an essential ingredient in pharmaceutical products. In this work, a method was developed for the quantitative and qualitative determination of 1,8-cineole using gas chromatography with tandem mass. The same technique was employed for detrmination of the concentrations of 1,8-cineole in the essential oils of cajeput, myrtle and niauli were determined. Triple quadeupole mass spectrometer was used for monitoring different 1,8-cineole signals in MRM mode for specific transition reactions. Thus, the mass spectrometry was optimized by determining the collision energies with nitrogen for each selected transition. The concentration range of 50 µg mL -1 - 2000 µg mL -1 was used to create calibration curves. The tested parameters of the evaluation of the method (accuracy, precision, specificity, linearity, limits of determination and proof) were satisfactory. By analyzing real samples of essential oils using the mentioned method, their concentrations were successfully determined.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:167:961037
Study programmeTitle: Chemistry
Study programme type: university
Study level: undergraduate
Academic / professional title: sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije (sveučilišni/a prvostupnik/prvostupnica (baccalaureus/baccalaurea) kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
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Created on2023-01-18 10:01:14