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master's thesis
Priprava senzora od ugljikove paste s NPOE kao vezivom i NaTPB kao taložnim reagensom
diplomski rad
2021. urn:nbn:hr:167:186992
Pašalić, Klara
University of Split
Faculty of Chemistry and Technology
Division of Chemistry

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Pašalić, K. (2021). Priprava senzora od ugljikove paste s NPOE kao vezivom i NaTPB kao taložnim reagensom : diplomski rad (Master's thesis). Split: University of Split, Faculty of Chemistry and Technology. Retrieved from https://urn.nsk.hr/urn:nbn:hr:167:186992

Pašalić, Klara. "Priprava senzora od ugljikove paste s NPOE kao vezivom i NaTPB kao taložnim reagensom : diplomski rad." Master's thesis, University of Split, Faculty of Chemistry and Technology, 2021. https://urn.nsk.hr/urn:nbn:hr:167:186992

Pašalić, Klara. "Priprava senzora od ugljikove paste s NPOE kao vezivom i NaTPB kao taložnim reagensom : diplomski rad." Master's thesis, University of Split, Faculty of Chemistry and Technology, 2021. https://urn.nsk.hr/urn:nbn:hr:167:186992

Pašalić, K. (2021). 'Priprava senzora od ugljikove paste s NPOE kao vezivom i NaTPB kao taložnim reagensom : diplomski rad', Master's thesis, University of Split, Faculty of Chemistry and Technology, accessed 16 November 2024, https://urn.nsk.hr/urn:nbn:hr:167:186992

Pašalić K. Priprava senzora od ugljikove paste s NPOE kao vezivom i NaTPB kao taložnim reagensom : diplomski rad [Master's thesis]. Split: University of Split, Faculty of Chemistry and Technology; 2021 [cited 2024 November 16] Available at: https://urn.nsk.hr/urn:nbn:hr:167:186992

K. Pašalić, "Priprava senzora od ugljikove paste s NPOE kao vezivom i NaTPB kao taložnim reagensom : diplomski rad", Master's thesis, University of Split, Faculty of Chemistry and Technology, Split, 2021. Available at: https://urn.nsk.hr/urn:nbn:hr:167:186992

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Metadata
TitlePriprava senzora od ugljikove paste s NPOE kao vezivom i NaTPB kao taložnim reagensom : diplomski rad
Title (english)Preparation of carbon paste sensor with NPOE as binder and NaTPB as sedimentary reagent : master thesis
AuthorKlara Pašalić
MentorMarija Bralić (mentor)
Committee memberJosipa Giljanović (predsjednik povjerenstva)
Committee memberAnte Prkić (član povjerenstva)
Committee memberMarija Bralić (član povjerenstva)
GranterUniversity of Split
Faculty of Chemistry and Technology
(Division of Chemistry)
Split
Defense date and country2021-10-27, Croatia
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract
Pripravljena je i opisana ionsko-selektivna elektroda na bazi ugljikove paste za maprotilin hidroklorid (MAP), tetraciklički antidepresiv. Modificirana CPE temelji se na ugljikovoj pasti i maprotilin tetrafenilboratu (MAPTPB) otopljenim u 2-nitrofelinil octileteru (NPOE) kao tekućini za lijepljenje. Ukupan broj pripravljenih i testiranih membrana s različitim udjelima ugljika, NPOE i IAC-a je 18. Najbolje odzivne karakteristike pokazala je membrana 17 koja sadrži 48,87% grafita, 49,00% NPOE, 2,06% IAC-a i 0,07% NaTPB. Tako modificirana elektroda pokazala je Nernstov nagib od -59,14±1,98 mV po koncentracijskog dekadi u području linearnosti od 3,16 x 10 -6 do 3,16 x 10 -3 M . Vrijeme potrebno za uspostavu stabilnog odziva je oko 1 minute. Ovako pripravljeni senzor moguće je primijeniti na određivanje MAP-a u urinu.
Abstract (english)
An ion-selective electrode based on carbon paste for maprotiline hydrochloride (MAP), a tetracyclic antidepressant, was prepared and described. The modified CPE is based on carbon paste and maprotiline tetraphenylborate (MAPTPB) dissolved in 2-nitrophenyl octylether (NPOE) as a bonding fluid. The total number of prepared and tested membranes with different proportions of carbon, NPOE and IAC is 18. The best response characteristics were shown by membrane 17 containing 48.87% graphite, 49.00% NPOE, 2.06% IAC and 0, 07% NaTPB. The electrode thus modified showed a Nernst slope of -59.14 ± 1.98 mV per concentration decade in the linearity range of 3.16 x 10 -6 to 3.16 x 10 -3 M. The time required to establish a stable response is about 1 minute. 2-nitrophenyl octylether. The sensor prepared in this way can be used to determine the MAP in urine.
Keywords
Keywords (english)
Languagecroatian
URN:NBNurn:nbn:hr:167:186992
Study programmeTitle: Chemistry; specializations in: Environmental Protection, Organic Chemistry and Biochemistry
Course: Environmental Protection
Study programme type: university
Study level: graduate
Academic / professional title: magistar/magistra kemije (magistar/magistra kemije)
Type of resourceText
File originBorn digital
Access conditionsOpen access
Embargo expiration date: 2022-02-20
Terms of useLicence In copyright icon
Created on2021-12-20 09:32:05